Research

Research

Experimental Techniques

Thin film deposition, ceramic synthesis, and materials processing methodologies

DC and RF Sputtering

Physical vapour deposition of metallic and oxide thin films using direct-current and radio-frequency magnetron sputtering systems for precise compositional control.

Pulsed Laser Deposition (PLD)

KrF excimer laser system for growth of high-quality epitaxial and polycrystalline oxide thin films on various substrates under controlled oxygen partial pressure.

Solid-State Reaction Method

Conventional solid-state reaction route for bulk ceramic fabrication with controlled atmosphere sintering up to 1600 °C for complex oxide systems.

Ball Milling — Oxide Nanoparticles

High-energy planetary ball milling for synthesis and size reduction of oxide nanoparticles with controlled morphology and crystallite size distribution.

Sol-Gel Technique

Wet-chemical synthesis for nanoparticles, ceramics, and thin-film precursor preparation with compositional homogeneity at the molecular level.

Chemical Vapour Decomposition

Chemical vapor deposition (CVD) is a process used to produce high-quality, high-performance solid materials, such as thin films and coatings. It involves exposing a substrate to volatile gaseous precursors that react or decompose on the heated surface to form the desired solid deposit

Ferroelectric tester

Ferroelectric tester is used to measure and analyze the electrical properties of ferroelectric materials, such as polarization, coercive field, and hysteresis behavior. It helps to evaluate material performance for applications in memory devices, sensors, and actuators.

LCR meter

An LCR meter is widely used in dielectric studies to measure a material’s capacitance, inductance, and resistance across different frequencies. By analyzing these parameters, researchers can determine dielectric constant, loss tangent, and other electrical properties essential for understanding insulating and ferroelectric materials.

Characterization Techniques

Structural, optical, electrical, and biological characterization tools employed in the laboratory

X-Ray Diffraction (XRD)

Structural characterization including phase identification, lattice parameter determination, and Rietveld refinement for phase-pure ceramic and thin-film samples.

SEM & AFM — Morphology

Scanning electron microscopy and atomic force microscopy for surface morphology, grain size analysis, roughness measurement, and nanoscale topographical imaging.

Optical Properties

UV-Vis-NIR spectrophotometry and photoluminescence spectroscopy for band gap determination, transmittance studies, and optical characterization of thin films and nanoparticles.

Dielectric Properties

Frequency- and temperature-dependent dielectric permittivity and loss tangent measurements for ceramic and thin-film capacitor structures across a broad spectral range.

Ferroelectric Properties

Polarization–electric field (P-E) hysteresis loop measurements and leakage current analysis for evaluation of ferroelectric switching behaviour and remnant polarization.

Piezoelectric Properties

Direct and converse piezoelectric coefficient (d₃₃) measurement, electrostrain characterisation, and resonance-antiresonance analysis of piezoelectric ceramic actuators and sensors.

Electrical Properties

DC conductivity, current–voltage (I-V) characteristics, and Hall-effect measurements for carrier concentration and mobility determination in semiconductor and oxide thin films.

Impedance Spectroscopy

Broad-band complex impedance analysis from mHz to MHz for grain/grain-boundary conductivity separation, relaxation dynamics, and equivalent circuit modelling.

X-Ray Photoelectron Spectroscopy (XPS)

Surface elemental composition and chemical-state analysis of oxide thin films and ceramics; used for valence-state determination and binding-energy characterisation.

Raman Spectroscopy

Vibrational mode analysis for phase identification, structural phase transitions, oxygen vacancy studies, and strain characterisation in functional oxide systems.

Cell Culture Studies

In-vitro biocompatibility assessment of bioceramic scaffolds including cell viability, adhesion, and proliferation assays using osteoblast and fibroblast cell lines.

Lithography

Photolithographic and electron-beam lithographic patterning for micro- and nano-scale device fabrication, electrode definition, and thin-film sensor structuring.

Sponsored Research Projects

Externally funded projects from national agencies

# Project Title Sponsoring Agency Budget (₹ Lakhs) Duration Status
19 Pt/Magnetic Insulator Heterostructures for Efficient Spin Current Generation and Detection with Low-Dissipation Spin Transport ANRF 100.00 (1 Cr) In Progress Ongoing
18 Development of Indigenous Ceramic Discs for Thin Film Deposition Applications (Startup Proposal) IITG Technology Innovation & Development Foundation 60.00 Ongoing Ongoing
17 Synthesis of Hydroxyapatite Nanoparticles for Bio-medical & AlN Ceramics for Semiconductor Applications M/s Chemdist Membrane Systems Pvt Ltd 13.00 28/02/2022 – 27/02/2024 Completed
16 Exploring the Novel Piezoelectric Ternary Nitride System for Realizing Efficient High-Temperature Ultrasonic Transducer and AE Sensors (Co-PI) STARS 45.00 01/04/2024 – 31/05/2027 Ongoing
15 Development of Corrosive-Resistant Coatings for Underwater Applications IITG Technology Innovation & Development Foundation 50.00 30/11/2022 – 29/11/2025 Ongoing
14 Smart Wearable Advanced nanoSensing Technologies in Healthcare ASICs (SWASTHA) (Co-PI) MeitY, Govt. of India 4000.00 (40 Cr) 01/04/2022 – 31/03/2026 Ongoing
13 Indian Nanoelectronics Users Program Idea to Innovation (INUP–i2i) (PI) MeitY, Govt. of India 1000.00 (10 Cr) 01/09/2021 – 31/08/2024 Completed
12 Development of Indigenous Ceramic Discs for Sputter Sources and Electronic Applications DSIR & MOST 10.00 31/08/2022 – 31/12/2023 Completed
11 Development of Low Loss Ni-Zn Ferrite for High Power Circulators ISRO 37.00 23/09/2021 – 31/03/2024 Completed
10 Development of Biologically Active Ferroelectric Ca₁₀(PO₄)₆(OH)₂–(K₀.₅Na₀.₅NbO₃) Composite Thin Films for Biomedical Applications DST Core Grant 57.40 01/12/2019 – 31/03/2022 Completed
9 Development of Pill Box Type RF Window Based on AlN Ceramics for 3.7 GHz BRNS 35.75 01/04/2018 – 31/03/2020 Completed
8 Development of (K,Na)NbO₃ Ceramics Modified with LiTaO₃ and LiNbO₃ for Piezo and Pyroelectric Sensor Applications BRNS 35.00 01/04/2015 – 31/03/2018 Completed
7 Dielectric and Thermal Characterization of Mg(Zr₀.₀₅Ti₀.₉₅)O₃ Ceramics for Microwave Window Applications BRFST 45.00 01/09/2012 – 31/03/2016 Completed
6 Preparation and Characterization of Mg₂TiO₄ Ceramics by Mechanical Alloying DRDO 17.00 01/01/2010 – 31/03/2013 Completed
5 Fabrication of K₀.₅Na₀.₅NbO₃ Ferroelectric Thin Film Capacitors by RF Magnetron Sputtering (Young Scientist Research Award) BRNS 18.00 01/01/2011 – 31/03/2014 Completed
4 Deposition and Characterization of BNW Films for CMOS Applications (Young Scientist Research Award) DST-SERB 15.00 01/01/2012 – 31/03/2015 Completed
3 Preparation and Characterization of Barium Zinc Tantalate Films for Complementary Metal Oxide Semiconductor Applications IIT Guwahati 6.20 01/10/2010 – 31/03/2013 Completed
2 FIST Program 2009, Phase I DST 150.00 2010 – 2015 Completed
1 FIST Program 2016, Phase II DST 400.00 2015 – ongoing Completed

Major Proposals from Centre for Nanotechnology

Large-scale funded and submitted proposals under national programmes

MeitY · Approved

Indian Nanoelectronics Users Program — Idea to Innovation (INUP–i2i)

Approved under MeitY, Govt. of India. Officiating PI: HoC, Centre for Nanotechnology. Project Execution PIs: Prof. D. Pamu, Dr. S. Akshai Kumar (Chemistry), Dr. M. Arun Tej (EEE). Co-PIs: Members of Nanotechnology Centre.

Approved Grant: ₹10 Crore  ·  Agency: MeitY, Govt. of India  ·  Approved

MeitY · Phase II Submitted

Centre for Excellence in Research and Development of Nanoelectronic Theranostic Devices

Proposal for a Centre of Excellence focused on research and development of nanoelectronic devices for theranostic (therapy + diagnostics) biomedical applications. Phase II submitted to MeitY, Govt. of India.

Proposed Grant: ₹20 Crore  ·  Agency: MeitY, Govt. of India  ·  Phase II Submitted

DST · Submitted

Multifunctional Nanomaterials based Point-of-care Diagnostics, Sensors and Energy Conversion Devices

Submitted to DST for Centre for Excellence in Nanomaterials. Collaborative proposal with Prof. S. C. Sharma, VC Tumkur University, and Dayananda Group Institutions.

Proposed Grant: ₹20 Crore  ·  Agency: DST  ·  Submitted

DST · Submitted

National Initiative for Developing and Harnessing Innovations (NIDHI)

Proposal submitted to DST under the NIDHI (National Initiative for Developing and Harnessing Innovations) programme for fostering innovation and technology translation from the Centre for Nanotechnology, IIT Guwahati.

Proposed Grant: ₹6 Crore  ·  Agency: DST  ·  Submitted to DST

Startup Proposals

Technology translation and entrepreneurship initiatives emerging from laboratory research

PRISM · DSIR

Indigenous Ceramic Discs for Sputter Sources

Development of indigenous ceramic discs for sputter sources and electronic applications. Submitted for financial support to the Dept. of Scientific and Industrial Research (DSIR) under the PRISM scheme — Promoting Innovations in Individuals, Start-Ups, and MSMEs.

INUP-i2i · Startup

M/s DSP Innovations — Sputtering Targets

Process development for sputtering targets and ceramic discs proposed as a startup under the INUP-i2i programme in the name of M/s DSP Innovations, leveraging indigenous manufacturing capabilities developed at IIT Guwahati.

Bio Nest · Incubation

Hybrid Ferroelectric Thin Films for Biomedical Applications

Development of hybrid electrically active biocompatible ferroelectric thin films for biomedical applications. To be incubated under the Bio Nest programme from the Centre for Nanotechnology, IIT Guwahati.

Research Facilities

Major equipment and instruments available in the Condensed Matter Physics Laboratory

Single Target RF Magnetron Sputtering System

For deposition of single-component oxide and metallic thin films. Make: Advanced Process Technology, India.

Dual Target RF Magnetron Sputtering System

Enables sequential or alternating deposition from two targets for multilayer thin-film structures. Make: Advanced Process Technology, India.

Three Target RF Magnetron Co-Sputtering System

Simultaneous co-sputtering from three targets for complex multi-component oxide thin-film growth. Make: Advanced Process Technology, India.

LCR Meter (20 Hz – 1 MHz)

Dielectric measurements with temperature variation from 25 °C to 500 °C for ceramic and thin-film samples. Make: Wayne Kerr Electronics, UK.

Krupka Resonant Cavity — Bulk Microwave Measurements

Precision microwave characterization of bulk ceramic substrates using resonant cavity method. Make: QWED, Poland.

Split Post Dielectric Resonators (5, 10 & 15 GHz)

Multi-frequency dielectric characterization of substrates and thin films at 5, 10, and 15 GHz. Make: QWED, Poland.

Planetary Ball Mill

High-energy milling for oxide nanoparticle synthesis and ceramic powder preparation with controlled particle size. Make: Fritsch GmbH, Germany.

KBr Press

Hydraulic pellet press for preparation of KBr discs and ceramic pellets for FTIR and dielectric measurements. Make: Technosearch Instruments, India.

High Temperature Furnace

Programmable sintering furnace for high-temperature oxide ceramic processing with controlled heating profiles. Make: Lenton, UK.

Microwave Sintering Furnace

Rapid, energy-efficient microwave sintering of ceramic compacts with uniform volumetric heating. Make: Enerzi Heating Reinvented, India.

Impedance Material Analyzer (1 MHz – 3 GHz) [CIF]

Broadband impedance analysis with temperature variation from −140 °C to 400 °C for dielectric relaxation studies. Make: Agilent Technologies & Novocontrol, Germany.

Ferroelectric Tester

P-E hysteresis loop, fatigue, retention, and imprint measurements for ferroelectric ceramic and thin-film capacitor characterization. Make: Radiant Technologies, USA.

DC Poling Setup

High-voltage DC poling of piezoelectric and ferroelectric ceramic samples for domain alignment and piezoelectric activation. Make: Marine, India.

pH Meter

Precision pH measurement for sol-gel and wet-chemical synthesis processes during nanoparticle and ceramic precursor preparation. Make: Eutech Instruments, Singapore.

LCR Meter (20 Hz – 2 MHz)

Dielectric and impedance measurements with temperature variation from 25 °C to 100 °C for thin-film and device characterization. Make: Keysight, USA.